Compound 5-Ho
[{(C5Me4SiMe3Ho)4(μ-H)5}(μ-H)4MoC5Me5]
From: Molecular heterometallic hydride clusters composed of rare-earth and d-transition metals
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InChIKey QTIGKOSWHSJFRW-UHFFFAOYSA-N
Compound data: CIF
Synthetic procedure: See article for the definitive version of this procedure and for full experimental details.
Similar to the preparation of 5 described above, heating 3a-Ho·C7H8 (50 mg, 0.028 mmol) under vacuum afforded 5-Ho·C7H8 (43 mg, 0.024 mmol, 86%) as black crystals. Anal. calcd for C58H108MoSi4Ho4·C7H8: C, 44.22; H, 6.62. Found: C, 44.30; H, 6.93.
