Abstract
GENERAL methods for preparation of organo–tin compounds of divalent tin have been reviewed by Gilman et al.1. The most usual methods include reaction of stannous chloride with a Grignard reagent or lithium alkyl and reduction of a dialkyl tin IV dichloride with sodium amalgam. In addition, reaction of sodium triethoxyl-alumino hydride with organo–tin IV halides in certain circumstances leads to formation of divalent organo–tin compounds2.
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References
Ingham, R. K., Rosenberg, S. D., and Gilman, H., Chem. Rev., 60, 459 (1960).
Schnitz-Dumont, O., and Bungard, G., Chem. Ber., 92, 2399 (1959).
Chem. Abstracts, 53, 9061 (1959).
Brit. Patent, No. 802, 796.
Krause, E., and Becker, R., Ber., 53, b, 173 (1920).
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SMITH, T. Reaction of Di-isobutyl Aluminium Hydride with Stannic Chloride. Nature 199, 374–375 (1963). https://doi.org/10.1038/199374a0
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DOI: https://doi.org/10.1038/199374a0
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