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| Open AccessThe moment of initial crystallization captured on functionalized nanoparticles
Understanding the mechanism of supercooling suppression by crystallization seeds is important for designing semiclathrate hydrates for latent heat storage materials. Here, we show that 10-30 nm cluster formation around silver nanoparticles promotes crystallization of supercooled aqueous solutions.
- Hironobu Machida
- , Takeshi Sugahara
- & Izumi Hirasawa
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Article
| Open AccessPhysical and chemical imaging of adhesive interfaces with soft X-rays
Understanding adhesion mechanisms for polymer composites is challenging due to the bonded interface being buried. Here, soft X-rays are used to probe the chemical and physical nature of the interface, revealing multiscale factors that influence the adhesion mechanism and bond strength.
- Hiroyuki Yamane
- , Masaki Oura
- & Takaki Hatsui
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Article
| Open AccessFast in-situ X-ray scattering reveals stress sensitivity of gypsum dehydration kinetics
Understanding the dehydration of gypsum is important for fluid-triggered earthquakes, and for its use in the construction industry. Here, x-ray scattering reveals that a small elastic load substantially accelerates dehydration kinetics, and is far more effective than applying heat.
- Christoph Eckart Schrank
- , Oliver Gaede
- & Andrzej P. Radliński
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Article
| Open AccessRedox-structure dependence of molten iron oxides
Knowing the atomic structure of liquid iron oxide is key to understanding steelmaking processes and magma flows. Here, Fe-O atomic coordination numbers are determined during levitation melting at a range of temperatures and oxygen partial pressures, revealing low coordination numbers.
- Caijuan Shi
- , Oliver L. G. Alderman
- & Chris J. Benmore