Compound I

9-(1,7-Dicarba-closo-dodecaboranyl)thiol

From: A coordination chemistry dichotomy for icosahedral carborane-based ligands

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InChIKey ODAJIIFYGIXASI-UHFFFAOYSA-N

Synthetic procedure: See article for the definitive version of this procedure and for full experimental details.

Compound I was prepared according to a literature procedure (Zakharkin, L. I. & Pisareva, I. V. Preparation of bis(o- and m-carbonyl)disulfides under the effect of sulfur chlorides on o- and m-carboranes in the presence of aluminum chloride. Izv. Akad. Nauk SSSR, Ser. Khim. 12, 2794-2796 (1981). English translation of this article: Russ. Chem. Bull. 12, 2328-2330 (1981)).