Abstract
PRICE1 reports an anomalous band at about 1,250 cm.−1 in the paraffin-oil mull spectrum of lithium borohydride at room temperature. This band does not occur in the room-temperature spectra of sodium borohydride2,3 and potassium borohydride3 or in the low-temperature spectra of sodium borohydride2,4 and potassium borohydride (Schutte, C. J. H., unpublished results).
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References
Price, W. C., J. Chem. Phys., 17, 1044 (1949).
Schutte, C. J. H., Spectrochim. Acta, 16, 1054 (1960).
Waddington, T., J. Chem. Soc., 4783 (1958).
Schutte, C. J. H., thesis, University of Amsterdam (1960).
Harris, P. M., and Meibohm, E. P., J. Amer. Chem. Soc., 69, 1231 (1947).
Halford, R. S., J. Chem. Phys., 14, 8 (1946).
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SCHUTTE, C. The BH4 − Ion in the Lithium Borohydride Lattice. Nature 189, 745–746 (1961). https://doi.org/10.1038/189745b0
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DOI: https://doi.org/10.1038/189745b0
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