Abstract
The need for more accessible energy resources makes shale formations increasingly important. Characterization of such lowpermeability formations is complicated, due to the presence of multiscale features and defies conventional methods. Highquality 3D imaging may be an ultimate solution for revealing the complexities of such porous media, but acquiring them is costly and time consuming. Highquality 2D images, on the other hand, are widely available. A novel threestep, multiscale, multiresolution reconstruction method is presented that directly uses 2D images in order to develop 3D models of shales. It uses a highresolution 2D image representing the smallscale features to reproduce the nanopores and their network, a large scale, lowresolution 2D image to create the largerscale characteristics and generates stochastic realizations of the porous formation. The method is used to develop a model for a shale system for which the full 3D image is available and its properties can be computed. The predictions of the reconstructed models are in excellent agreement with the data. The method is, however, quite general and can be used for reconstructing models of other important heterogeneous materials and media. Two biological examples and from materials science are also reconstructed to demonstrate the generality of the method.
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Introduction
Due to the substantial amount of natural gas that they store, shales have emerged as one of the most promising current and future energy resources. Shale gas can be dissolved in kerogen, be adsorbed on clay and kerogen, and/or appear as free gas in pores and natural fractures^{1,2}. Most of the gas production in such porous formations occurs in the source area because, owing to the low permeability of the formations^{3}, the gas does not migrate significantly.
Unlike conventional largescale reservoirs that have been characterized through countless methodologies^{4}, shale formations have not yet undergone advanced characterization and much remains to be done. A most important obstacle to characterization and modeling of shales, which up to now has seemed insurmountable, is their multiscale structure that defies the conventional techniques of characterization. Pores of all sizes, ranging from nano to micro exist in shales^{5,6}, which play a vital role in fluid flow^{7,8}. The intrinsic small scale and spatial variability of such pores require a very large number of samples for direct characterization of shales that, if available, will make it possible to better understand the depositional environment, mineralogy, maturation, thermal condition, total organic carbon, strain/stress properties, porosity and permeability of shales. But, shales are also largescale porous media and, therefore, the spatial variations of their properties also occur not only at very large scales. Thus, there are several distinct and disparate length scales that are relevant to modeling and characterization of shales.
Two or threedimensional (3D) imaging of shale samples have become an important tool for their characterization, because they reveal very useful information about their pore network and their spatial connectivity and provide a reliable platform for their characterization. In addition, some of the aforementioned key morphological and flow properties of shales, such as the TOC, mineralogy, porosity, permeability and other physical properties can be extracted using such images^{9}. As a result, the acquisition of highresolution 2D and 3D images through the use of focused ionbeam scanning electron microscopes^{10} (FIBSEM) is viewed an essential part of such studies. While highresolution 2D images can be obtained with relative ease, acquisition of 3D images that are necessary for precise characterization is costly and time consuming. Furthermore, some information, such as pore spots, can be lost during layer milling^{10}. Thus, obtaining highquality 3D images has become an outstanding challenge.
Given the availability of 2D images, reconstructing a representative 3D sample using such images would be very efficient, costeffective and beneficial. Acquiring and processing a 2D SEM image takes minutes to hours and costs hundreds of dollars, whereas processing a 3D FIBSEM image takes days and costs tens to hundreds of thousands of dollars. Another disadvantage of the FIBSEM images is their tiny size—tens of nanometers edge size—compared with the 2D SEM images that can be as large as hundreds of micrometers in edge. Because of the labor, cost and limited size, if one can develop a technique to use only 2D images, then there would be no need to fully scan a sample in 3D when a few 2D images or even one single, relatively large 2D image can convey even more information about the heterogeneity and morphology of the sample.
Some efforts in this direction have been made. Slatt, O’Brien and coworkers^{11,12,13} proposed a method for using 2D SEM images of shales, obtained from carefullybroken clean 2D shale surface of a cubic sample. For each surface several separate viewing areas are selected at random and photographed and are then used to estimate the sample’s various properties. Several magnifications of the images are used to estimate the properties at different “scales,” and in particular the “area” porosity, i.e. the porosity based on surface not volume of a sample. The method can yield important insights into the structure of shales at small scales.
Several statistical methods are also available that extract the important statistics/properties and then generate stochastically many realizations of the formation^{14,15,16,17}. Typically, such methods are based on an optimization technique, such as simulated annealing, by which one minimizes the differences between the inferred statistical properties from the initial dataset and those in the simulated model. The extracted statistics using such methods are, however, poor and fail to reproduce a highquality model. In another group that is process based, one tries to mimic the real physical process to develop a model^{18,19,20}. Such methods are not computationally feasible. They also require considerable calibrations due to the extreme heterogeneity and variability of shale formations and do not represent a general approach as each method is developed for a specific type of porous media. In addition, most of the current methods are based on some loworder statistical descriptors that cannot reproduce the complex structures that are abundant in shales. Moreover, they are unable to use directly qualitative information, such as insight into the type of structure that a given formation may be expected to have. Consequently, all the necessary details of the physical process and morphological information must first be “extracted” and then “translated” numerically and even then only some of the information can be used effectively. Statistically, reproducing longrange connected features that are important to flow and transport is not possible using a limited number of data points. Generating such features requires processing a large amount of data over extended length scales (i.e., higherorder statistics) at the same time. Providing such “large data sets” is not, however, feasible in the earth sciences and, in particular, for modeling of largescale porous media.
All the aforementioned shortcomings can be addressed using a conceptual data set called a digital image, which represents auxiliary information that brings in the effect of the physical process and extra supplementary data that can be used in the framework of highorder statistics, in order to develop an accurate model. The digital image can simply be the result of processbased processes that have given rise to the formation, or a SEM image. Once the image is available, an important and heretofore unexplored approach to modeling of shales can be developed, which is based on reconstruction: Given a certain amount of data, one tries to reconstruct a model for shales that not only honors the data, but also provides accurate predictions for those properties for which there are no data or, if such data are available, they are not used in the reconstruction.
The aim of this paper is to propose a new, accurate and efficient reconstruction method for modeling multiscale heterogeneous media using 2D SEM images. The method reconstructs the corresponding 3D model for a shale formation using the 2D images. Unlike previous methods, the available dataset is used directly in the proposed method, thereby eliminating the need for data extraction. We show how to avoid taking a large number of costly and timedemanding highresolution 2D images and, instead, use a combination of just a few low and highresolutions images to rapidly reconstruct models of 3D shales. To our knowledge, the present work is the first study on shale reconstruction that reduces the cost and time tremendously. The results of this study can be used for accurate modeling of fluid flow and transport in such complex largescale porous media. Most importantly, as we demonstrate in the supplementary information, the method is general and may be used to reconstruct 3D models of a wide variety of heterogeneous materials and media
Results and Discussion
To test the methodology, a highly complex sample is selected. The 3D image of the sample is available; see Fig. 1(a). Thus, we first use the 3D image of the sample to compute its permeability and porosity. After the 3D model of the sample is reconstructed based on 2D images, a comprehensive comparison of its flow and physical parameters with those of the original 3D sample is presented.
Reconstructed model
To apply the method to a difficult but also realistic problem, a minimum amount of information for the sample, namely, two images, one high resolution and a second one with low resolution are extracted from the 3D image. Figure 1(b) depicts the largescale pores that are the main flow paths in the shale, representing the lowresolution image. Figure 1(c) represents the highresolution image that exhibits nanoscale pores, distributed between the large channels, which play an important role in connecting the largescale pores.
The nanoscale shale sample contains two very different pore structures that are at two separate scales. Therefore, the proposed multiscale approach is implemented for the sample as follow: First, the representative image shown in Fig. 1(c) that depicts the finescale nanopores is used to stochastically reconstruct several realizations using the method described below. One reconstructed realization is presented in Fig. 2(a). Then, using the lowresolution digital image in Fig. 1(b), the largescale pores are reconstructed; see Fig. 2(b). Finally, the reconstructed models for the two disparate scales are superimposed to achieve a single model; see Fig. 2(c). It is clear that the largescale model reproduces the main features of the pore space at the corresponding scales, while the paths are connected through the nanopores. We now compare the properties of the reconstructed models with those of the original 3D sample.
The autocorrelation function and probability distribution
The porepore autocorrelation function is defined by
where r_{i} indicates the spatial location within the model and is an indicator, such that if r_{i} is in the pore space and otherwise. is the porosity. The autocorrelation functions of the original sample and the reconstructed models were computed for three orthogonal directions and shown in Fig. 3. Clearly, the two sets of results agree. The accuracy of the autocorrelation function is not, however, sufficient for verifying the accuracy of the reconstructed models.
Using the probability distribution of the pixels as a separate constraint improves the reproduction of the nano and micropores. Naturally, since we use the crosscorrelation simulation (CCSIM) algorithm to begin the reconstruction (as described below) that uses a crosscorrelation function representing higherorder statistics of the formation, we expect the probability distribution to be reproduced. However, the exact distribution of the original 3D sample might not be reproduced due to utilizing one 2D image to reconstruct the 3D formation. Thus, the probability distributions of several realizations are compared with that of the original 3D sample; see Fig. 4. The complex multimodal probability distributions are well reproduced.
Multiplepoint connectivity probability
The comparisons so far involved lowerorder statistical properties that only account for a probability/occurrence of the individual points. Largescale connectivity is one of the most important properties that should be reproduced, as it controls flow in porous media^{4}. In particular, multiplepoint connectivity is^{21} concerned with the probability p(r; m) of having a sequence of m points connected in a given phase of a multiphase material (e.g. pore and matrix) in a direction r. It is defined by
where is the indicator function of phase i defined earlier. p(r;m) accounts for the global connectivity of a system and represents a strict test of the reconstruction method’s accuracy. The results are shown in Fig. 5. The agreement between the computed probabilities of the original 3D sample and the generated stochastic models is excellent.
Effective permeability
Despite the high accuracy of the reproduced statistical properties described so far, they are still insufficient for asserting that the reconstructed model is accurate, because it is possible for two media to have similar statistics for their morphological properties, but very different flow characteristics. Therefore, we present a comparison between the flow properties of the original samples and those of the generated 3D models.
The original 3D image contains 4000 × 4000 × 1800 voxels. The effective permeability K_{e} is a measure of the ability of a pore space for fluid flow. Due to the extreme spatial heterogeneity and anisotropy associated with the samples, a single effective permeability cannot realistically characterize the flow property of a large shale sample. Therefore, the directional effective permeabilities were calculated for three orthogonal directions and regions within the 3D sample, using commercial software Avizo®. To obtain estimates of the range of the possible variations of K_{e}, several smaller pieces of the 3D images were used to compute the effective permeabilities. Avizo® was also used for the permeability calculations of the reconstructed samples. In all cases, the Stokes’ equation,
was solved numerically, assuming that the fluid is incompressible and Newtonian and the flow is at steady state and in the laminar regime. Here, p is the pressure of the fluid, v is its velocity and is its dynamic viscosity. The noslip condition at porefluid interfaces was assumed. A pressure difference of 3 × 10^{4} Pa (upstream = 13 × 10^{4} Pa and downstream = 10 × 10^{4} Pa) and a fluid viscosity of 0.001 Pa.s were used in the calculations. The results are presented in Fig. 6, indicating very good agreement with results of the original 3D samples.
Conclusions
Realistic models of complex porous media cannot be developed based on loworder statistics alone. In particular, if they represent multiscale systems with distinct, disparate and relevant length scales and heterogeneities at all the scales, one needs an approach that utilizes higherorder statistics and information at all the relevant scales by a computationallyaffordable method. Shale formations represent an important class of such porous media. This paper presented a multiscale, multiresolution method for reconstructing models of highly complex porous media and demonstrated its accuracy for a shale sample. The method combines several elements: an iterative 3D reconstruction, a probability distribution matching, a multiresolution algorithm and a multiscale approach. The iterative algorithm removes the possible artifacts during the initial reconstruction process. The probability distribution matching prevents artificial smoothness and guarantees an accurate reproduction of the complex multimodal shale distribution. The intrinsic multiscale pore structures in shale formations are reproduced using two efficient methods, namely, multiscale and multiresolution imaging. Altogether, the new technique presented in this paper is able to accurately reproduce the complex pore features in shale samples. It can be used as a tool for reducing the cost and time in the studies of shale and related structure for which highquality 3D images are required.
Multiscale materials and media are abundant in nature and occur widely in other fields, such as biology, nanotechnology and materials science. The method presented here can also be used to model such materials and media as well. Three examples to which the proposed method was applied are provided in the Supplementary Information. Therefore, the method is not restricted to the shales considered in this paper and can provide models for other important heterogeneous media and materials for which one has a few high and lowresolution 2D images and the aim is to generate 3D models for them.
Methodology
The proposed methodology consists of three steps. Each step relies on the model developed in the previous steps and improves it.
Step 1
This step utilizes the cross correlationbased simulation (CCSIM) method, which belongs to a class of stochastic models that aims to produce an ensemble of equiprobable realizations^{22} of disordered media, such as porous formations. The method is cast on a computationally fast crosscorrelation formulation that allows achieving efficient and accurate modeling in a very short time. First, a representative 2D image is selected as the digital image; see Fig. 7(a). The image must contain most of the expected features, including the connectivity and distribution of the pores, the porosity and other important factor and is set as the first layer (external surface) at the bottom of the 3D model, represented by a 3D cubic computational grid G. Then, five frames that, together with the digital image form the six orthogonal outside surface of the model are, reconstructed based on the CCSIM algorithm (see below). The reconstruction is conditional, i.e. each frame is reconstructed subject to honoring the data at the interface between itself and the already existing frames. Thus, the first reconstructed layer honors the data at its interface with the digital image, the next frame honors the data at its interface with any of the existing frames (including the digital image, if applicable) and so on.
As shown in Fig. 7, the CCSIM algorithm reconstructs the system conditionally and plane by plane, after doing so for the first five external frames or planes. The 2D computational grid (plane) is partitioned into small blocks called templates T, while the data event at position u in T is denoted by D_{T}(u), so named to signify the fact that it can change during the reconstruction. Every two neighboring templates share an overlap region. Then, the other four frames (i.e. left, right, front and back) are reconstructed, starting from a corner of the grid G and proceeding along a 1D raster path, as shown in Fig. 7. At each step, to preserve the continuity between the patterns in the neighboring blocks, an overlap region is considered and its similarity to the entire digital image is calculated using the following crosscorrelation function:
where and and represents the location at point of the digital image that is used to reconstruct a target system of size , with and . The overlap region of size is used to match the pattern in the selected block with the digital image. Any realization of an overlap region with a crosscorrelation function larger than a threshold is an acceptable pattern. Finally, one of the acceptable patterns in the ensemble of the realizations is selected at random and inserted in the current data event D_{T} in the computational grid G.
Since the reconstruction of each layer (plane) is conditional, optimal locations of the hard data—those that must be honored exactly—in the already reconstructed layers must be specified. Each layer is conditioned to the hard data in the immediately reconstructed layer before it and to the data at its interfaces with the four external frames (reconstructed at the beginning) that it touches. The hard data must be selected from the immediatelyreconstructed layer. To do so, we use the Shannon entropy S: For each template of the immediatelyreconstructed layer the entropy S is computed. Since a more heterogeneous template has higher entropy, the template is split recursively if S is high. The splitting continues until the right template size—one that contains low entropy—is generated. Next, a fraction of the hard data in the final template with the lowest entropy is selected and the next layer is reconstructed. Finally, all the generated layers are stacked together to build the 3D model. Clearly, one can generate as many realizations as needed. Note that different digital images can be selected on the basis of the sample’s complexity and heterogeneity. For example, various digital images for illustrating the vertical, horizontal and lateral directions can be utilized.
Step 2
The complete continuity of the reconstructed model is sometimes not achievable by Step 1 and the generated realizations may contain some artifacts. Thus, the model in Step 1 is further improved using an iterative scheme to minimize the discontinuities and reproduce patterns that are even more similar to those in the digital image, while preserving their continuity. To this end, the 3D model reconstructed in Step 1 is further refined voxel by voxel. A voxel in the 3D model and three orthogonal patterns around it are selected from the 3D model; see Fig. 8. Then, the crosscorrelation functions between the patterns and the 2D digital images are computed and, in each plane, the closest patterns , i.e. those for which the crosscorrelation functions are the largest, are selected. An average of the selected patterns is assigned to the selected voxel. The averaging might, however, produce artifacts resulting in a 3D model that may be too smooth and not suitable for computing the flow properties, because the low and highpermeability areas have been averaged out. We will come back to this issue shortly.
Step 3
As mentioned, shale formations exhibit a sharp bimodal distribution of pore sizes^{9,23}. Nano and microscale pore structures are very common in shales and both features should appear in a realistic model for them. Indeed, it has been demonstrated through laboratory experiments that the nanopores along microspores’ networks control gas transport^{1,7,24}, as they provide the connection between them. Thus, their presence, representing an interconnected pore network, is very important. The largescale structures make up the main pore network, even though they are connected through the nanopores. Since having a highquality 2D image of a large sample is not feasible due to its high cost and timedemanding processing, it is preferable to take two images with different resolutions: (a) one large 2D lowresolution image for capturing the microscale structure, which is easily obtained and (b) one or a few small 2D highresolution images for taking into account the structure of the nanopores’ network. The two sets of images are viewed as complementary datasets for revealing the main structures within a shale sample. To address these issues, three complementary methods are presented and utilized: a probability distribution matching and a multiresolution approach, both combined with a multiscale method.
Probability distribution matching
Reproducing the multimodal pore structure is an important issue, not only in shales, but also in most earth science problems. For example, most largescale porous media contain a broad permeability distribution. In such porous media the emphasis is on the highpermeable zones. Due the overall low permeability of shales, however, all the smallscale features are also important and must be included in the final model.
The probability distribution matching provides a method to control the patterns in the 3D model that was produced by Steps 1 and 2 and helps one to select one of the candidate patterns more efficiently. The probability distribution of the voxels in the 3D model of Steps 1 and 2 (M) is constructed after the candidate patterns in Step 2 are selected. Then, a “distance” , where DI represents the digital image, is calculated between the resulting probability distribution of each new 3D model using the candidate pattern . The distance (i.e. the difference) between the two distributions is quantified using the JensenShannon divergence theorem, which is the average of two KullbackLeibler divergences^{25,26},
and is always positive. Finally, the central voxel of the pattern that has the minimum is selected as the final one in M. This concept is illustrated in Fig. 9. Conditioning the final 3D model to the probability distribution of the digital image helps one to reproduce both the global structure and the statistical properties. The probability distribution brings both nano and microscale pores into the final model. Furthermore, the issue of generating a too smooth of a model by using an average as the final pixel value is resolved using this algorithm.
Multiresolution properties
One of the most common properties of shales, indicated by highquality SEM images, is the simultaneous presence of nano and microscale pore networks that significantly affects the properties of the formation. Current methodologies must be adjusted accordingly to handle very large datasets provided by the SEM images. Thus, a multiresolution approach for addressing such deficiencies as computational cost and pattern reproduction is described.
The idea is based on a pyramid representation of a large dataset—a digital image in this case. In this method, the original large digital image is upscaled (coarsened) into successive images with fewer blocks or templates using a nearestneighbor algorithm; see Fig. 10. The coarsened block that represents m × m pixels in the finerscale blocks is assigned the same pixel value as the one among the m × m pixels with the highest probability. This avoids generating a smooth upscaled images, most of which fall within the range and distribution of the original digital image due to the nearestneighbor algorithm. After the images are prepared at various scales (different block sizes), the algorithm is applied as follows: first, the overlap region in the 3D model G, reconstructed so far, is resized according to the coarsest available block in the digital image. In other words, if we upscale the digital image into a smaller number of larger blocks by reducing the number of the small blocks by a factor f, we do the same with the overlap region. Then, the location of the matching pattern is marked on the coarsest digital image, L = 3 in Fig. 10. Next, the identified location is projected onto the finer digital image and a small window is searched to determine the matching pattern in the finerscale digital image; see L = 2 in Fig. 10. Using the small search window decreases the computational demands tremendously, because (a) it is not necessary to search the entire next finer digital images and (b) a lower resolution image provides roughly the same information as that of the large digital image. The process is continued until the final resolution, L = 0 in Fig. 10, is reached. The selected pattern at this level is inserted directly in the model. It should be noted that the original digital image can be upscaled until it keeps the same amount of information as the fineresolution one (i.e. the digital image is not coarsened excessively). In this paper, three levels L are used. This multiresolution approach is particularly useful for problems in which the initial digital image is very large and the upscaling does not change enormously the details of the main features. Fortunately, most of currentlyavailable shale images are taken using highresolution imagining tools and, thus, our technique for reducing the computational burden will be very cost effective.
The multiresolution approach reduces the processing time and preserves the important features effectively. It allows the algorithm to use large templates, thereby producing a better model of large and highlyconnected structures and works well for multimodal shale samples.
Mutiscale properties
Depending on their resolution, each of the available imaging tools reveals some information at a specific scale^{27}. For example, the widely available 2D/3D lowresolution microtomography images depict largescale structures. Such images are insufficient for accurate pore space modeling of shales because they cannot display an interconnected pore network. Submicron (nanoscale) images are needed for obtaining a reliable estimation of the permeability and other physical parameters. But, as pointed out earlier, obtaining a large number of highresolution 2D/3D FIBSEM images is not affordable. Thus, various images having different resolution and revealing some specific information should be used. Therefore, a methodology that can use the multiscale information and reconstruct a model that contains the statistics of various sources is highly important. The multiscale images depict the final pore network.
Suppose that in addition to the highresolution digital image used so far, we also have a lowresolution image at larger scale. Then, in addition to the highresolution 3D model reconstructed so far, we reconstruct a 3D model based on the lowresolution image. Finally, the final multiscale pore network is obtained by overlaying the microscale (highresolution) and macroscale (lowresolution) 3D models. One can generate many stochastic macroscale 3D models, if the available 3D macroscale image is not representative. It is also worth mentioning that this technique can be used with nonstationary systems even when various datasets need to be integrated^{28,29}.
Additional Information
How to cite this article: Tahmasebi, P. et al. Multiscale and multiresolution modeling of shales and their flow and morphological properties. Sci. Rep. 5, 16373; doi: 10.1038/srep16373 (2015).
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Acknowledgements
Work at USC was supported in part by the RPSEA Consortium and at the University of Texas at Austin by the NanoGeosciences lab. We would like to thank the FEI Company for use of Aviso®. We also would like to thank Professor Mohammad Piri of the University of Wyoming for providing us with the SEM dataset.
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The three authors conceived the problem. P.T. developed the method and performed the computations. All authors contributed to analyzing the results. P.T. and M.S. wrote the manuscript.
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Tahmasebi, P., Javadpour, F. & Sahimi, M. Multiscale and multiresolution modeling of shales and their flow and morphological properties. Sci Rep 5, 16373 (2015). https://doi.org/10.1038/srep16373
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DOI: https://doi.org/10.1038/srep16373
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