Abstract
Vinylidene chloride-butyl acrylate copolymers were prepared by photopolymerization at room temperature. The molecular weight of these copolymers have been determined using Gel Permeation Chromatography and the copolymer composition estimated using Schoneger technique. 2D NMR techniques such as 1H-13C heteronuclear single quantum correlation (HSQC) was used for the compositional and configurational assignments of 1H and 13C{1H} NMR spectra for various resonating signals. 2D 1H homonuclear double quantum filter-correlated spectroscopy (DQF-COSY) is used to get better insight for the copolymer structure.
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Brar, A., Malhotra, M. Comprehensive Assignments of 1H and 13C NMR Signals for the Vinylidene Chloride-Butyl Acrylate Copolymers Using 2D NMR Spectroscopy. Polym J 30, 513–519 (1998). https://doi.org/10.1295/polymj.30.513
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DOI: https://doi.org/10.1295/polymj.30.513