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Article
Nature Nanotechnology 1, 131–136 (1 November 2006) | doi:10.1038/nnano.2006.95
Size-selective growth of double-walled carbon nanotube forests from engineered iron catalysts
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Abstract
We have succeeded in synthesizing vertically aligned doubled-walled carbon nanotube (DWNT) forests with heights of up to 2.2|[nbsp]|mm by water-assisted chemical vapour deposition (CVD). We achieved 85|[percnt]| selectivity of DWNTs through a semi-empirical analysis of the relationships between the tube type and mean diameter and between the mean diameter and the film thickness of sputtered Fe, which was used here as a catalyst. Accordingly, catalysts were engineered for optimum DWNT selectivity by precisely controlling the Fe film thickness. The high efficiency of water-assisted CVD enabled the synthesis of nearly catalyst-free DWNT forests with a carbon purity of 99.95|[percnt]|, which could be templated into organized structures from lithographically patterned catalyst islands.
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