Abstract
The encapsulation of poly (n-butyl acrylates) (PBA) onto carbon black (CB) surface via ultrasonic irradiation initiating emulsion polymerization was investigated. The results showed that the route performed at ambient temperature can efficiently prepare PBA encapsulated CB as proved by the aggregation of PBA encapsulated CB in the precipitator of PBA. The surface properties of CB coated with PBA were analyzed by FT-IR and XPS. The content of PBA encapsulated on the CB surface reaches 11.87% determined by TGA. Compared with the conventional chemical modification of CB, it was found that the particle size of CB obtained by the present approach can be controlled, and dynamic light scattering results quantified that CB particles with narrower size distribution and smaller size were obtained. The PBA encapsulated CB can be dispersed uniformly in the polymer matrix.
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Li, Q., Wu, G., Zhang, X. et al. Preparation of Poly (n-butyl acrylates) Encapsulated Carbon Black via Ultrasonic Irradiation Initiating Emulsion Polymerization. Polym J 38, 1245–1250 (2006). https://doi.org/10.1295/polymj.PJ2006053
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DOI: https://doi.org/10.1295/polymj.PJ2006053
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