Abstract
WE have already described1 the use of a high resolution NMR spectrometer for recording 31P, NMR spectra of solids and pointed out some advantages and limitations of the method. We now report the use of this technique in elucidating unequivocally the solid state structures of dibromo and diiodotriphenylphosphorus(V) which have not been determined before2. The structure of dibromotriphenylphosphorus(V) in nitrobenzene solution is also discussed.
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DILLON, K., WADDINGTON, T. Structures of Some Dihalotriphenylphosphorus(V) Compounds. Nature Physical Science 230, 158–159 (1971). https://doi.org/10.1038/physci230158b0
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DOI: https://doi.org/10.1038/physci230158b0
