Table 1 The up-scaled synthesis of imines and amides in the VFD housing a standard 18 cm long glass tube, entries 1–3, or a 38 cm long glass tube, entries 4–6 (both tubes 20 mm O.D.).
From: Neutron imaging and modelling inclined vortex driven thin films
Entry | Compound | Conversion | Yield | Production rate (g/hr) |
---|---|---|---|---|
1 |
![]() | 82% | 82% | 92 |
2 |
![]() | 87% | 45% | 62 |
3 |
![]() | 92% | 83% | 86 |
4 |
![]() | — | 48% | 38 |
5 |
![]() | — | 26% | 22 |
6 |
![]() | — | 28% | 22 |