Table 1 Data collection and refinement statistics

From: A family of unconventional deubiquitinases with modular chain specificity determinants

  ZUFSP S-SAD ZUFSP native
Data collection
Space group P6522 P6522
Unit cell constants
a, b, c (Å) 84.2, 84.2, 201.8 84.2, 84.2, 201.8
\(\alpha , \; \beta , \, \gamma\) (°) 90, 90, 120 90, 90, 120
Wavelength (Å) 2.07 0.98
Resolution (Å) 59.13–2.3 (2.38–2.3) 49.45–1.73 (1.79–1.73)
No. of observations 4,098,044 (364,012) 484,411 (48,504)
No. of unique reflections 35,609 (3576)a 44,866 (4337)
Multiplicity 115.1 (101.8) 10.8 (11.2)
Completeness (%) 100 (100) 100 (99)
Rmerge (%) 11.7 (39.5) 8.4 (82.4)
Rmeas (%) 11.8 (39.7) 14.3 (86.4)
<I/\(\sigma\)(I)> 47.7 (13.9) 16.6 (2.5)
CC1/2 (%) 100 (99.7) 99.8 (79.5)
Anomalous signal   
CCano (59.13–3 Å [3.08–3.0 Å]) (%) 56 (31)  
Rpim (59.13– 3 Å [3.08–3.0 Å]) (%) 0.8 (1.4)  
Refinement
Reflections used in refinement   44,862
Number of test reflections   1930
Rwork/Rfree (%)   17.8/20.7
Root-mean-square deviations
Bond lengths (Å)   0.005
Bond angles (°)   0.6
Average B factor (Å2)
All macromolecule atoms   37.0
Solvent molecules   39.5
Other atoms   24.3
Ramachandran plot (%)
Most favored   97.7
Additionally allowed   2.2
Disallowed   0.0
  1. aFriedel pairs were kept separate