Fig. 7 | Nature Communications

Fig. 7

From: Iron-based nanocatalyst for the acceptorless dehydrogenation reactions

Fig. 7

Synthesis of precursor (4) for nM5- lipoxygenase inhibitor. a Reaction conditions: To a 20 mmol of benzyl azide (in dichloromethane) was added TfOH (1.1 equiv.) followed by 4-fluorostyrene (2.0 equiv.) at 0 °C and allowed to stir for 1 h. b Reaction conditions: 3 (0.2 mmol), cat. Fe-L1@EGO-900 (8 mol%), t-BuOK (10 mol%), and mesitylene (2 mL) heated at 145 °C for 24 h

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