A commercial atomic force microscope can be used to image solid surfaces in liquids and measure interfacial energies with atomic resolution.
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Ruediger, A., Rosei, F. AFM extends its reach. Nature Nanotech 5, 388–389 (2010). https://doi.org/10.1038/nnano.2010.112
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DOI: https://doi.org/10.1038/nnano.2010.112