In an identification parade of chemical reactions using a single-electrode system, the charges generated by the mechanical rubbing of insulators are shown to be electrons rather than ions.
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Otero, T. Electrons create a reaction. Nature Mater 7, 429–430 (2008). https://doi.org/10.1038/nmat2188
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DOI: https://doi.org/10.1038/nmat2188