Table 1 Data collection and refinement statistics.

From: Ankyrin-mediated self-protection during cell invasion by the bacterial predator Bdellovibrio bacteriovorus

  Bd3460 native Bd3460 iodine derivative Bd3459 K38M,S70A variant Bd3459:Bd3460 complex Bd0816:Bd3460 complex Bd3459:Bd3460 PenG
Accession code 5CEA 5CEB 5CEC 5CER 5CED
Data collection
 Space group P212121 P212121 P1 P212121 P21212 P212121
 Cell dimensions
a, b, c (Å) 57.43, 99.64, 173.70 57.13, 99.18, 173.33 55.93, 65.04, 73.82 51.61, 59.17, 192.27 212.32, 237.45, 90.90 51.54, 59.16, 192.04
α, β, γ(°) 90, 90, 90 90, 90, 90 63.89, 83.27, 83.20 90, 90, 90 90, 90, 90 90, 90, 90
 Resolution (Å) 1.85 (1.95–1.85)* 2.4 (2.53–2.4) 1.93 (1.98–1.93) 1.36 (1.4–1.36) 2.48 (2.54–2.48) 2.02 (2.07–2.02)
Rsym 7.0 (49.3) 6.3 (31.0) 3.6 (76.6) 3.2 (51.6) 15.6 (75.3) 6.7 (67.2)
Rpim 6.0 (42.9) 1.6 (26.7) 2.5 (54.9) 2.0 (41.9) 4.6 (21.5) 3.1 (30.8)
 CC 1/2 0.99 (0.65) 0.99 (0.79) 0.99 (0.78) 0.99 (0.78) 0.99 (0.85) 0.99 (0.80)
I,/σI 10.0 (2.5) 34.4 (2.7) 16.2 (1.6) 23.4 (2.4) 15.1 (3.8) 16.2 (2.8)
 Completeness(%) 99.0 (100.0) 89.5 (47.8) 85.7 (79.2) 97.2 (77.8) 99.0 (99.5) 99.9 (99.9)
 Redundancy 3.8 (3.7) 13.9 (2.0) 3.8 (3.7) 6.0 (3.7) 13.5 (14.0) 6.5 (6.7)
Refinement
 Resolution (Å) 1.85 1.93 1.36 2.48 2.02
Rwork/Rfree 17.8/21.0 19.8/23.2 14.3/16.9 21.7/24.9 17.3/20.7
 r.m.s. deviations
Bond lengths (Å) 0.017 0.016 0.011 0.014 0.014
Bond angles (°) 1.75 1.63 1.44 1.68 1.60
  1. *Values in parentheses are for highest resolution shell.
  2. CC 1/2 is the correlation coefficient between two random half data sets.