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Conv., conversion; LA, lactic acid; TON, turnover number.
Reaction conditions: 3.78 g glycerol, 3 μmol 6 (0.007 mol%), 15 h (TON calculated for LA formation by 1H NMR spectroscopy using internal standard and confirmed by gas evolution quantified by gas burette measurements). Reactions carried out under N2 atmosphere and overall mass balance over 99%, unless otherwise noted. Maximum theoretical TON ~13,700.
*Reaction carried out in air.
†Reaction carried out under nitrogen and exposed to air after 10 min.