Compound 5-Dy
[{(C5Me4SiMe3Dy)4(μ-H)5}(μ-H)4MoC5Me5]
From: Molecular heterometallic hydride clusters composed of rare-earth and d-transition metals
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InChIKey BXOPLNFTAOWJKZ-UHFFFAOYSA-N
Compound data: CIF
Synthetic procedure: See article for the definitive version of this procedure and for full experimental details.
Similar to the preparation of 5 described above, heating 3a-Dy·C7H8 (40 mg, 0.023 mmol) under vacuum afforded 5-Dy·C7H8 (30 mg, 0.017 mmol, 74%) as black crystals. Anal. calcd for C58H108MoSi4Dy4·C7H8: C, 44.46; H, 6.61. Found: C, 44.56; H, 6.51.
