Abstract
WORK on the crystal structures of peroxochromates has been going on in this-laboratory for some years. The addition compound CrO5.C5H5N was prepared according to Hofmann and Hiendlmaier1 and was recrystallized in ether, which yielded well-developed needle-like crystals. The compound decomposed in one or two days. CrO5.C5H5N was investigated by the usual X-ray methods. It was found to have monoclinic symmetry, corresponding to the non-centro-symmetric space group P21 (No. 4).
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References
Hofmann, K. A., and Hiendlmaier, H., Ber., 38, 3066 (1905).
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STOMBERG, R. Crystal Structure of Peroxochromates, CrO5.C5H5N. Nature 196, 570–571 (1962). https://doi.org/10.1038/196570b0
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DOI: https://doi.org/10.1038/196570b0
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