Supplementary information

From the following article:

Synthesis of the H-cluster framework of iron-only hydrogenase

Cédric Tard, Xiaoming Liu, Saad K. Ibrahim, Maurizio Bruschi, Luca De Gioia, Siân C. Davies, Xin Yang, Lai-Sheng Wang, Gary Sawers and Christopher J. Pickett

Nature 433, 610-613(10 February 2005)

doi:10.1038/nature03298

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Supplementary Methods

Experimental, ESMS and PES information.

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Supplementary Notes

Note on dissociation step in Supplementary Figure 4.

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Supplementary Figure 1

X-ray structure of B.

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Supplementary Figure 2

PES spectrum of [Fe4S4(SEt)3{Fe2(CH3C(CH2S)3)(CO)5}]2-.

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Supplementary Figure 3

Simulation 10th scan of D.

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Supplementary Figure 4

Proposed mechanism for electrochemistry of D.

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Supplementary Figure Legends

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Supplementary Data

Crystallographic data of B.

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