Kidney International (1978) 13, 344–360; doi:10.1038/ki.1978.53
Physicochemical aspects of urolithiasis
Birdwell Finlayson1
1Division of Urology, Department of Surgery, University of Florida, College of Medicine, Gainesville, Florida
Correspondence: Dr Birdwell Finlayson, Division of Urology, Department of Surgery, University of Florida, College of Medicine, Gainesville, Florida 32610, U.S.A.
Top of pageAbstract
The following discussion centers on calcium oxalate and calcium phosphate stones, but permits generalization to other forms of stone. Although it constitutes a primer on the subject, it does attempt to deal with inconsistencies in our current meager knowledge of the physical characteristics of urolithiasis. In addition, it describes concepts and approaches that appear to be useful and that should be incorporated into urolithiasis research, to make future work in the field susceptible to analysis by conventional physical theory.
The known physicochemical features of urolithiasis are readily divided into four interrelated subjects: the driving force (supersaturation), nucleation, the growth of crystals and particles, and aggregation.
Top of pageReferences
- Nielsen AE: Kinetics of Precipitation. New York, Pergamon Press, 1964, p. 3
- Davies CW: Ion Association. London, Butterworths, 1962
- Robinson RA, Stokes RH: Electrolyte Solutions. London, Butterworths, 1959
- Robertson WG: Measurement of ionized calcium in biological fluids. Clin Chim Acta 24:149–157, 1969
- Pak CYC, Chu S: A simple technique for the determination of urinary state of supersaturation for brushite. Invest Urol 11:211–215, 1972
- Gill WB, Silvert MA, Roma MS: Supersaturation levels and crystallization rates of calcium oxalate from urines of normal humans and stone formers determined by a 14C-oxalate technique. Invest Urol 12:203–209, 1974
- Finlayson B: Calcium stones: Some physical and clinical aspects, Chapter 10, in Calcium Metabolism in Renal Failure and Nephrolithiasis, edited by David DS, New York, John Wiley, 1977
- Robertson WG, Peacock M, Marshall RW, Marshall DH, Nordin BEC: Saturation-inhibition index as a measure of the risk of calcium oxalate stone formation in the urinary tract. N Engl J Med 294:249–252, 1976 | PubMed | ChemPort |
- Finlayson B, Smith A: Spectrophotometry of the stability constant of CaC2O4 based on competition between murexide and oxalate for Ca2+. J Eng Chem Data 18:368–370, 1973
- Marshall RW, Robertson WG: Nomogram for the estimation of the saturation of urine with calcium oxalate, calcium phosphate, magnesium ammonium phosphate, uric acid, sodium acid urate, ammonium acid urate, and cystine. Clin Chim Acta 72:253–260, 1976
- Pak CYC, Hayashi Y, Finlayson B, Chu S: Estimation of the state of saturation of brushite and calcium oxalate in urine: A comparison of three methods. J Clin Lab Invest 89:891–901, 1977
- Pak CYC, Arnold L, Holt K, Cox C, Barilla D: Mechanisms for calcium urolithiasis among patients with hyperuricosuria. J. Clin Invest 59:426–431, 1973
- Sears GW: Influence of adsorbed films on crystal growth kinetics. J Phys Chem 25:154–159, 1958
- Ohata M, Pak CYC: The effect of diphosphonate on calcium phosphate crystallization in urine in vitro. Kidney Int 4:401–406, 1973 | PubMed | ISI | ChemPort |
- Pak CYC, Ohata M, Holt K: Effect of diphosphonate on crystallization of calcium oxalate in vitro. Kidney Int 7:154–160, 1975 | PubMed | ISI | ChemPort |
- Erwin D, Roberts JA, Sledge G, Bennett DJ, Finlayson B: Estimating urine supersaturation: A comparison of the result of two methods of evaluating changes induced by drinking milk, in Urolithiasis Research, edited by Fleish H, Robertson WG, Smith LH, Vahlensieck W, New York, Plenum, 1976, pp. 261–264
- Pak CYC: Quantitative assessment of various forms of therapy for nephrolithiasis in urinary calculi, in Stone Research, edited by Cifuentes-Delatte L, Rapado A, Basal, Karger, 1972, pp. 177–187
- Burdette WG, Thomas WC, Finlayson B: Urinary super-saturation with calcium oxalate before and during orthophosphate therapy. J Urol 115:418–422, 1976
- Robertson WG, Peacock M, Nordin BEC: Activity products in stone forming and non-stone forming urine. Clin Sci 34:579–594, 1968 | ISI |
- Walton AG: The Formation and Properties of Precipitates. New York, Interscience Publishers, 1961
- Sears GW: The origin of spherulites. J Phys Chem 65:1738–1741, 1961
- Walton AG: Nucleation in liquids and solids, Chapter 5, in Nucleation edited by Zottlemeyer AC, Marcel Decker, 1969
- Turnbull D, Vonnegut B: Nucleation catalysis. Indust Eng Chem 44:1292–1298, 1952 | ISI | ChemPort |
- Lonsdale K: Epitaxy as a growth factor in urinary calculi and gallstones. Nature 217:56–58, 1968 | Article | PubMed | ISI | ChemPort |
- Venables JA, Price GL: Nucleation of thin films, in Epitaxial Growth, edited by Matthews JW, New York, Academic Press, 1975, p. 429
- Murphy BT, Pyrah LH: The composition, structure and mechanisms of the formation of urinary calculi. Br J Urol 34:129–185, 1962
- Keith HD, Padden FJ: A phenomenological theory of spherulitic crystallization. J Appl Phys 34:2409–2421, 1963 | Article | ISI | ChemPort |
- Uhlmann DR, Chalmers B: The energetics of nucleation. Indust Eng Chem 57:19–31, 1965
- Garten VA, Head RB: Nucleation in salt solutions. J Chem Soc [Perkin I] 69:514–520, 1973
- Robertson WG: A method for measuring calcium crystalluria. Clin Chim Acta 26:105–110, 1969
- Johnson RT, Rousseau RW, McCabe WL: Factors affecting contact nucleation. Am Inst Chem Eng Symposium Series 68:31–41, 1972
- DeBoer JH: The Dynamical Character of Adsorption. Oxford, The Clarendon Press, 1953, Chapter 1
- Trump BF, Dees JH, Kim KM: Some aspects of kidney structure and function with comments on tissue calcification in the kidney, in Urolithiasis, edited by Finlayson B, Hench L, Smith LH, Washington, D.C., National Academy of Science, 1972, p. 1
- Malek RS, Boyce WH: Intranephronic calculosis: Its significance and relationship to matrix nephrolithiasis. J Urol 109:551–555, 1973 | PubMed | ISI | ChemPort |
- Nielsen AE: The kinetics of electrolyte precipitation. J Colloid Sci 10:576–586, 1955
- Coe FL, Lawton RL, Goldstein RB, Tembe V: Sodium urate accelerates precipitation of calcium oxalate in vitro. Proc Soc Exp Biol Med 149:926–929, 1975 | PubMed | ISI | ChemPort |
- Pak CYC, Hayashi Y, Arnold LH: Heterogeneous nucleation of calcium oxalate by seeds of monosodium urate. Proc Soc Exp Biol Med 149:930–932, 1975
- Meyer J, Bergert J, Smith LH: Epitaxy in the calcium phosphate-calcium oxalate crystal growth systems, in International Colloquium on Renal Lithiasis, edited by Thomas WC, Finlayson B, Gainesville, Fla., University of Florida Press, 1976, pp. 66–76
- Pak CYC, Hayashi Y, Arnold LH: Heterogeneous nucleation with urate, calcium phosphate and calcium oxalate. Proc Soc Exp Biol Med 153:83–87, 1976 | PubMed | ISI | ChemPort |
- Finlayson B, Miller GH: An analysis of experimental foreign body stone formation. J Theor Biol 23:344–346, 1969
- Robertson WG, Peacock M, Nordin BEC: Calcium crystalluria in recurrent renal stone formers. Lancet 2:21–24, 1969 | PubMed | ChemPort |
- Doremus RH, Gardner GL, McKay W: Crystallization of calcium oxalate in various media and urolithasis, in International Colloquium on Renal Stones, edited by Thomas WC, Finlayson B, Gainesville, Fla., University of Florida Press, 1976, pp. 18–32
- Nancollas GH, Gardner GL: Kinetics of crystal growth of calcium oxalate monohydrate. J Cryst Growth 21:267–276, 1974
- Johnson RA, O'Rourke JD: The kinetics of precipitate formation: Barium sulfate. J Am Chem Soc 76:2124–2131, 1954
- Füredi-Milhofer H, Purgaric B, Bre
evi
L, Pavkovi
N, Oljica E: Nucleation of calcium phosphate from solutions at physiological pH. Croatica Chem Acta 41:37–42, 1969 - Marshall RW, Nancollas GH: The kinetics of crystal growth of dicalcium phosphate dihydrate. J Phys Chem 73:383–384, 1969
- Meyer JL, Smith LH: Growth of calcium oxalate crystals: I. A model for urinary stone growth. Invest Urol 13:31–35, 1975
- Finlayson B: Where and how does urinary stone disease start? An essay on the expectation of free-and-fixed particle urinary stone disease, in International Bladder Stone Conference Proceedings, Bethesda, Maryland, National Institutes of Health, Fogarty Center for International Studies, 1976, pp. 7–32
- Tomazi
B, Nancollas GH: The seeded growth of calcium phosphates: Surface characterization and the effect of seed material. J Coll Interface Sci 50:451–461, 1975 - Finlayson B: The concept of a continuous crystallizer. Invest Urol 9:258–263, 1972
- Randolph AD, Larson MA: Theory of Particulate Processes, Analysis and Techniques of Continuous Ciystallization. New York, Academic Press, 1971
- Miller JD, Randolph AD, Drach GW: Some observations of calcium oxalate crystallization in urine-like mother liquors, in International Colloquium on Renal Lithiasis, edited by Thomas WC, Finlayson B, Gainesville, Fla., University of Florida Press, 1977, pp. 33–40
- Miller JD: Crystallization kinetics of calcium oxalate in simulated urine. Ph.D. Thesis, University of Arizona, 1976
- LeGeros R, Morales P: Renal stone crystals grown in gel systems. Invest Urol 11:12–16, 1973
- Bisaillon S, Tawashi R: Growth of calcium oxalate in gel systems. J Pharm Sci 64:458–460, 1975
- Rumpf H, Schubert H: Adhesion forces in agglomeration processes, in Sciences of Ceramic Processing Before Firing, edited by Onoda G, Hench L, New York, John Wiley and Sons Publishers, 1977
- Meyer AS, Finlayson B, DuBois L: Direct observation of urinary stone ultrastructure. Br J Urol 43:154–163, 1971
- Leal J, Finlayson B: Adsorption of naturally occurring polymers on calcium oxalate surfaces. Invest Urol 14:278–283, 1977 | PubMed | ChemPort |
- Adamson AW: Physical Chemistry of Surfaces. New York, Interscience Publishers, 1970
- Overbeek JTG: Kinetics of flocculation, in Colloid Science, edited by Kyrut HR, Elsevier Press, 1952, pp. 278–301
- Meyer JL, Smith LH: Growth of calcium oxalate crystals: II. Inhibition by natural urinary crystal growth inhibitors. Invest Urol 13:36–39, 1974
- Meyer JL, McCall JT, Smith LH: Inhibition of calcium phosphate crystallization by nucleoside phosphates. Calc Tiss Res 15:287–293, 1974
- Robertson WG, Peacock M, Nordin BEC: Inhibitors of the growth and aggregation of calcium oxalate crystals in vitro. Clin Chim Acta 43:31–37, 1973 | PubMed |
- Robertson WG, Knowles F, Peacock M: Urinary acid mucopolysaccharide inhibitors of calcium oxalate crystallization, in Urolithiasis Research, edited by Fleisch H, Robertson WG, Smith LH, Vahlensieck W, New York, Plenum Press, 1976