Table 1
A hydrocarbon ruler measures palmitate in the enzymatic acylation of endotoxin
Victoria E Ahn, Eileen I Lo, Christian K Engel, Lu Chen, Peter M Hwang, Lewis E Kay, Russell E Bishop and Gilbert G Privé
- The EMBO Journal (2004) 23, 2931 - 2941
- doi:10.1038/sj.emboj.7600320
Published online: 22 July 2004
Back to article| Diffraction data | Native | NaBr | CsCl | SeMet |
|---|---|---|---|---|
| Resolution (Å) | 1.9 | 2.7 | 2.6 | 2.6 |
| Unit cell (Å) | ||||
| a,b | 50.67 | 51.02 | 51.12 | 50.60 |
| c | 158.44 | 158.31 | 158.23 | 158.06 |
| Wavelength (Å) | 0.9505 | 0.9050 | 0.9505 | 1.54 |
| Reflections collected | 227 607 | 48 970 | 71 093 | 49 340 |
| Unique reflections | 17 041 | 5967 | 6925 | 6217 |
| Completeness (%) | 99.5 (99.9) | 93.9 (94.5) | 99.0 (100.0) | 89.8 (93.4) |
 I / I | 38.1 (9.0) | 17.9 (5.6) | 21.2 (7.7) | 29.6 (4.2) |
| Rsym (%) | 5.0 (33.7) | 8.6 (45.2) | 7.8 (38.5) | 6.2 (39.8) |
| Refinement | Native | |||
| Resolution (Å) | 20.0–1.90 | |||
| Data cutoff F/(F) | 0 | |||
| R/Rfree, 5% (%) | 21.65/25.55 | |||
| R.m.s.d. bond lengths (Å) | 0.015 | |||
| R.m.s.d. bond angles (deg) | 1.44 | |||
| Number of atoms/residues | ||||
| PagP | 1225/157 | |||
| LDAO | 66/3 complete, 2 partial | |||
| Acetate | 20/3 | |||
| MPD | 16/2 | |||
| Waters | 38 | |||
| Numbers in parentheses refer to the highest resolution shell. | ||||
